Determination of Emamectin Benzoate in Medicated Fish Feed

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Determination of emamectin benzoate in medicated fish feed.

A method was developed to quantitate emamectin benzoate in fish feed at levels between 5 and 15 ppm. The active ingredient is extracted from 20 g medicated feed into aqueous-methanolic solvent by overnight shaking. A solid-phase extraction procedure using a 2 g C18 cartridge is then used to concentrate the active residue and remove interfering matrix components. The extracted drug and internal ...

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ژورنال

عنوان ژورنال: Journal of AOAC INTERNATIONAL

سال: 1999

ISSN: 1060-3271,1944-7922

DOI: 10.1093/jaoac/82.6.1281